Time:2023.02.08Browse:1
The alkaline acid method includes two reaction processes: alkali melting process and acid immersion process. The alkali melting process is to chemically react with the acidic impurities in the molten and graphite under high temperature conditions under high temperature conditions, especially silicon -containing impurities (such as silicate, silicone aluminate, quartz, etc.) to generate soluble salt, and then Remove impurities after washing and improve the purity of graphite. The basic principle of the acid immersion process is to use acid and metal oxide impurities reactions. This part of impurities did not respond to alkali during the alkali melting process. The metal oxide is converted into a soluble salt, and then washed to separate it from graphite. The combination of alkali melting and acid immersion has a good effect on the graphite.
A variety of alkaline substances can remove graphite impurities. The stronger the base, the better the purity effect. The alkali acid method is mostly naOH with small melting points and strong alkali. The acids used in the acid immersion process can be HCL, H2SO4, HNO3, or mixed between them, of which HCL has more applications.
For some high silicon -containing graphite, the purifying graphite of the alkali melting method can also achieve comprehensive recycling of silicon. The solution of the alkaline melting acid is acidic, and the silicon impurities in the solution will be transformed into silicic acid. A certain amount of alum can be extracted to extract silicic acid, and then a pure silicon dioxide can be obtained by a high temperature of 900 ° C.
The alkaline acid method is the most widely used method in the production of graphite purification industries in my country. It has the advantages of less one -time investment, high product quality, strong adaptability, etc., as well as the advantages of simple equipment and strong versatility. Definition is that high temperature burning, large energy consumption, long process process, severe equipment corrosion, large graphite loss, and severe wastewater pollution. Therefore, comprehensive utilization technologies such as polymer silicide and iron chloride are used to purify the wastewater.